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Pitting resistance equivalent number (PREN) is a predictive measurement of a stainless steel's resistance to localized pitting corrosion based on its chemical composition. In general: the higher PREN-value, the more resistant is the stainless steel to localized pitting corrosion by chloride.
PREN is frequently specified when stainless steels will be exposed to seawater or other high chloride solutions. In some instances stainless steels with PREN-values > 32 may provide useful resistance to pitting corrosion in seawater, but is dependent on optimal conditions. However, crevice corrosion is also a significant possibility and a PREN > 40 is typically specified for seawater service.[1][2][3]
These alloys need to be manufactured and heat treated correctly to be seawater corrosion resistant to the expected level. PREN alone is not an indicator of corrosion resistance. The value should be calculated for each heat to ensure compliance with minimum requirements, this is due to chemistry variation within the specified composition limits.
PREN formulas (w/w)
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There are several PREN formulas. They commonly range from:
to:
There are a few stainless steels which add tungsten (W), for those the following formula is used:
All % values of elements must be expressed by mass, or weight (wt. %), and not by volume. Tolerance on element measurements could be ignored as the PREN value is indicative only.
Pitting resistance measurement
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Exact pitting test procedures are specified in the ASTM G48 standard.[5]
References
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The first-generation Duplex stainless steels were developed more than 70 years ago in Sweden for use in the sulfite paper industry. Duplex alloys were originally created to combat corrosion problems caused by chloride-bearing cooling waters and other aggressive chemical process fluids.
Called Duplex because of its mixed microstructure with about equal proportions of ferrite and austenite, Duplex stainless steels are a family of grades, which range in corrosion performance depending on their alloy content. The term “Super-Duplex” was first used in the 1980’s to denote highly alloyed, high-performance Duplex steel with a pitting resistance equivalent of >40 (based on Cr% + 3.3Mo% + 16N%).
With its high level of chromium, Super-Duplex steel provides outstanding resistance to acids, acid chlorides, caustic solutions and other environments in the chemical/petrochemical, pulp and paper industries, often replacing 300 series stainless steel, high nickel superaustenitic steels and nickel-based alloys. The chemical composition based on high contents of chromium, nickel and molybdenum improves intergranular and pitting corrosion resistance. Additions of nitrogen promote structural hardening by interstitial solid solution mechanism, which raises the yield strength and ultimate strength values without impairing toughness. Moreover, the two-phase microstructure guarantees higher resistance to pitting and stress corrosion cracking in comparison with conventional stainless steels. From the introduction of its first-generation, Duplex steel has seen a steady increase in popularity. Recently, the production of highstrength, corrosion resistant super-duplex coil has been implemented in the marine and chemical industries, architecture and mast riggings, wire lines, lifting and pulley equipment and well service strands. In fact, development of wire processing techniques has enabled the production of steel wires down to 1mm in diameter.
Super-Duplex falls under the Duplex stainless steel grouping.
Duplex stainless steels are graded for their corrosion performance depending on their alloy content. Today, modern Duplex stainless steel can be divided into four groups:
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